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Trends in Organic Chemistry   Volumes    Volume 18 
Abstract
Comparing neat vs. solution reactions of chlorosulfonyl isocyanate with alkenes
Dale F. Shellhamer, Kelsey L. Alexander, Zachary J. Beavis, Marcela S. Bucardo, Sarah L. Elwin, Leticia Gomez, Christine J. Licata, Sara Van Horne, Marc C. Perry
Pages: 15 - 20
Number of pages: 6
Trends in Organic Chemistry
Volume 18 

Copyright © 2017 Research Trends. All rights reserved

ABSTRACT
 
Neat reactions of chlorosulfonyl isocyanate (CSI) with hydrocarbon alkenes and monofluoroalkenes in the presence of bicarbonate were compared to the maximized reaction conditions in solution. Electron-deficient alkenes react with CSI to give better product yields when reactions were carried out as neat mixtures. Electron-rich alkenes with CSI give good and comparable results when the reactions were run as either neat mixtures or in solution.
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