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Current Topics in Electrochemistry   Volumes    Volume 6 
Abstract
Pulse-electrolysis stopped-flow method for spectroscopic analyses of electrogenerated species
Satoshi Okazaki, Munetaka Oyama
Pages: 199 - 212
Number of pages: 14
Current Topics in Electrochemistry
Volume 6 

Copyright © 1998 Research Trends. All rights reserved

ABSTRACT
 
By connecting a column electrolysis method with a stopped-flow technique, a pulse-electrolysis stopped-flow method has been developed. This method has many advantages that it can be applied not only to the detection and characterization of unstable intermediates but also to the analysis of the reaction kinetics of heterogeneous electrode reactions as homogeneous reactions. In addition, this method can be utilized combined with various spectroscopic observations including UV-visible, resonance Raman (RR) and electrogenerated chemilumiluminescence (ECL) measurements. In this review, the advantages of this method are demonstrated with many successful results obtained using the pulse-electrolysis stopped-flow method.
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