ABSTRACT In our recent research, it was that the microwave irradiation method is one of the most promising techniques to fabricate the size-controlled organic nanocrystals. The fibrous nanocrystals of polydiacetylene could be obtained by using Teflon-sealed quartz vessel in this method for the purpose of keeping high temperature and pressure. The characteristic solid-state-polymerization behavior will be also described in polydiacetylene nanofibers.
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